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- W1986292807 abstract "Abstract Two inclusion compounds of the 11-[bis(p‐chlorophenyl)hydroxymethyl]-9,10-dihydro-9,10-ethanoanthracene host (1) have been studied by X-ray diffraction in order to find an explanation of the exceptional clathrate formation ability of the present chloro-containing host as compared with that of closely related chlorine-free host analogues. Crystal data: 1·ethyl acetate (2:1), C27H22OCl2·½(C4H8O2), Mw = 501.45, P21/c, a = 8.9060(5), b = 11.1109(6), c = 25.642(1) A, β = 99.03(1)°, Z = 4, R = 0.047 for 2029 F values with I>2σ(I); 1·cyclohexylamine (1:2), 2[C29H22OCI2·2(C6H13N)], Mw = 1311.50, Pc, a = 12.144(2), b = 12.689(3), c =23.119(8) A, β = 91.68(1)°, Z = 2, R = 0.054 for 3073 F values with I>2σ(I). Although the two solid inclusion compounds differ in host‐guest stoichiometry, space group symmetry and also in host‐guest recognition mode, both co-crystals are held together by numerous C‒H…X (X = O, N or Cl) interactions, in which the chloro-substituents of 1 play a very active role. The observed f..." @default.
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- W1986292807 date "1998-11-01" @default.
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- W1986292807 title "The Role of Chloro Substituents in Solid Inclusion Formation. Crystal Structures Formed by a Bulky Hydroxy Host with Ethyl Acetate (2:1) and Cyclohexylamine (1:2) as Guest" @default.
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- W1986292807 doi "https://doi.org/10.1080/10610279808055405" @default.
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