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- W1986473679 abstract "Neutron powder diffraction is used to determine the crystal structure of LiCD3COO · 2D2O at 293 and 1.5 K. Lithium acetate dihydrate crystallizes in theCmmmspace group in the room-temperature phase witha= 6.82082(9) Å,b= 10.88842(12) Å,c= 6.59911(7) Å, andZ= 4. The CH3groups are dynamically disordered, and there are short H bonds between the water molecules and the acetate oxygen atoms. There is a phase transition to a low-temperature modification which has the space groupPmanwitha= 6.70246(7) Å,b= 10.87932(11) Å,c= 6.56999(7) Å, andZ= 4. The CH3groups are ordered in this phase, but have large thermal ellipsoids even at 1.5 K. The H atoms of the water molecules also have large thermal ellipsoids even at 1.5 K, but the CH3group tunneling spectrum shows no evidence for coupling with the motions of the water molecules." @default.
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- W1986473679 date "1996-11-01" @default.
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- W1986473679 title "The Crystal Structure and Methyl Group Dynamics in the Room-Temperature and Low-Temperature Phases of Lithium Acetate Dihydrate" @default.
- W1986473679 doi "https://doi.org/10.1006/jssc.1996.0327" @default.
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