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- W1986649557 abstract "TiN nanopowder was synthesized by carbothermal reduction method by using a (TiO2 + C) precursor derived from titanyl nitrate, urea, glucose, ammonium nitrate, and citric acid mixed solution. The results revealed that the obtained precursor consisted of flake particles with a uniform dispersion of amorphous TiO2 and C. The precursor powders were subsequently calcined under nitrogen at 900–1300 °C for 2 h. The initial transformation of TiO2 to TiN, by adopting this route, occurred at 900 °C. Moreover, TiOxNy, TiO2, and carbon below 1200 °C, and TiCxNy, TiOxNy, TiO2, and carbon at (or above 1200 °C) were found to be as impurities with the calcined products. The lattice parameter of TiN synthesized at 1100 °C (α = 4.240 Å) agrees well with the theoretical value (α = 4.241 Å). TiN powder, synthesized at 1100 °C, exhibited well-distributed spherical particles ranging from 80 to 100 nm. The nitrogen, oxygen, and residual carbon contents of TiN powder synthesized at 1100 °C were found to be 20.37 wt.%, 1.91 wt.%, and 3.36 wt.%, respectively." @default.
- W1986649557 created "2016-06-24" @default.
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- W1986649557 date "2013-07-01" @default.
- W1986649557 modified "2023-10-18" @default.
- W1986649557 title "Preparation of TiN nanopowder by carbothermal reduction of a combustion synthesized precursor" @default.
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- W1986649557 doi "https://doi.org/10.1016/j.matchar.2013.04.010" @default.
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