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• W1986728712 abstract "Journal of Heterocyclic ChemistryVolume 9, Issue 1 p. 115-118 Note NMR spectral evidence for the 4-hydroxy-1-benzothiopyrylium ion† E. Campaigne, E. Campaigne Chemistry Laboratories of Indiana University, Bloomington, IndianaSearch for more papers by this authorS. W. Schneller, Corresponding Author S. W. Schneller Chemistry Laboratories of Indiana University, Bloomington, Indiana Taken in part from a thesis submitted in partial fulfillment of the requirements for the Ph. D. degree by S. W. S., Indiana University, June, 1968.Department of Chemistry, University of South Florida, Tampa, Florida 33620Search for more papers by this author E. Campaigne, E. Campaigne Chemistry Laboratories of Indiana University, Bloomington, IndianaSearch for more papers by this authorS. W. Schneller, Corresponding Author S. W. Schneller Chemistry Laboratories of Indiana University, Bloomington, Indiana Taken in part from a thesis submitted in partial fulfillment of the requirements for the Ph. D. degree by S. W. S., Indiana University, June, 1968.Department of Chemistry, University of South Florida, Tampa, Florida 33620Search for more papers by this author First published: February 1972 https://doi.org/10.1002/jhet.5570090119Citations: 6 † Contribution No. 1999 from the Chemical Laboratories of Indiana University. AboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onEmailFacebookTwitterLinkedInRedditWechat References 2 E. Campaigne, H. R. Burton, C. D. Blanton Jr. and S. W. Schneller, J. Heterocyclic Chem., 8, 65 (1971). 3 R. Zahradnik and J. Koutecky, Collect. Czech. Chem. Commun., 28, 1117 (1963). 4 T. Nozoe, “ Non-Benzenoid Aromatic Compounds,” D. Ginsburg, Ed., Interscience Publishers, Ltd., London, England, 1959, p. 343. 5 E. Campaigne and R. D. Hamilton, Quart. Rep. Sulfur Chem., 5, 275 (1970). 6 Personal communication with R. Zahradnik, Institute of Physical Chemistry, Czechoslovak Academy of Sciences, Prague, Czechoslovakia whose molecular orbital data is gratefully acknowledged. 7 F. Bossert, Ann. Chem., 680, 40 (1964). 8 R. H. Martin, N. Defay, F. Geerts-Evrard, P. H. Given, J. R. Jones, and R. W. Wedel, Tetrahedron, 21, 1833 (1965). 9 T. E. Young and C. J. Ohnmacht, J. Org. Chem., 32, 1558 (1967). 10 Another noteworthy observation but not directly related to the above discussion is the presence of a deshielding effect exerted by the 2-phenyl of VIII upon the 3-hydrogen in deuteriochloroform indicating that the 2-phenyl must possess some co-planarity with the entire ring system (e.g., i). 11 Spectra were determined on a Varian A-60 Spectrometer in deuteriochloroform and trifluoroacetic acid with tetramethylsilane as an internal standard at ambient probe temperatures. 12 Multiplicity designated as s, d, t, q and m represents singlet, doublet, triplet, quartet and multiplet, respectively. 13 Melting points were taken on a Mel-Temp capillary melting point apparatus and were corrected. The microanalyses were performed by Midwest Microlab, Inc., Indianapolis, Indiana. 14 F. Krollpfeiffer and H. Schultze, Ber., 56, 1819 (1923). 15 F. Arndt, Ber., 56, 1269 (1923). 16 C. D. Hurd and S. Hayao, J. Am. Chem. Soc., 76, 5065 (1954). 17 French Patent 1,365,504, July 3, 1964 to; J. R. Boissier and C. Malen, Chem. Abstr., 61, 14642d (1964). Citing Literature Volume9, Issue1February 1972Pages 115-118 ReferencesRelatedInformation" @default.
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• W1986728712 title "NMR spectral evidence for the 4-hydroxy-1-benzothiopyrylium ion" @default.
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