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- W1986852118 abstract "INVESTIGATION of the heats of interaction of cellulose with water and with aqueous solutions of electrolytes is one means of studying structural peculiarities of this polymer. In most cases the heats of interaction of cellulose materials with water were studied. Moreover there was only partial breakdown of the fibre structure: as has been shown by several methods, a characteristic of cellulose is the presence of segments tha t are largely or completely inaccessible to water. In view of this the data obtained could give no adequate idea of the structure of the material, or of the energies of interaction among cellulose macromolecules which determine the structural peculiarities of the material. The object of the present investigation was to s tudy the heats of interaction of cellulose with aqueous solutions of organic bases which cause the complete transition of cellulose into the dissolved state. In this case it is reasonable to expect the complete breakdown of the intermolecular bonds of the cellulose, and consequently free access for the interaction of hydroxyl groups of the cellulose with water. Secondary processes of formation of addition compounds of cellulose with the base should be of no real importance here. In particular this was shown in [1] where it was found that heats of mercerization were no more than 0.23 cal/g, i.e. quanti tat ively not comparable with the heats of cellulose hydration. EXPERIMENTAL" @default.
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- W1986852118 date "1967-01-01" @default.
- W1986852118 modified "2023-09-26" @default.
- W1986852118 title "Heats of interaction of cellulose fibres with basic solutions" @default.
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- W1986852118 doi "https://doi.org/10.1016/0032-3950(67)90405-4" @default.
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