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- W1987043670 abstract "Synthesis of methyl-N-phenyl carbamate from the oxidative carbonylation of aniline with methanol has been studied over CuCl2-NaI, PdCl2-NaI, PdCl2-CuCl2-NaI, and PdCl2-CuCl2-HCl in an autoclave at 373/438 K and 0.13/3.79 MPa. Carbamate yields decreased in the order: CuCl2-NaI>PdCl2-NaI>PdCl2-CuCl2-NaI>PdCl2-CuCl2-HCl at 438 K and 3.79 MPa. Product distribution profiles showed that carbamate yield increased with reaction time and leveled off at 43.5% over CuCl2-NaI after 1 h of batch reaction at 438 K and 3.79 MPa. The low cost and high activity of CuCl2-NaI could provide a novel and cost-effective process for carbamate synthesis." @default.
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- W1987043670 date "2003-03-01" @default.
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- W1987043670 title "CuCl2 and PdCl2 catalysts for oxidative carbonylation of aniline with methanol" @default.
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- W1987043670 doi "https://doi.org/10.1016/s1381-1169(02)00550-2" @default.
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