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- W1987187819 abstract "(Tetracyanonaphthalocyaninato)iron(II) with Isocyanides as Axial Ligands (Tetracyanonaphthalocyaninato)iron(II) [(CN) 4 ‐2,3‐NcFe; 6 ] is obtained by treating 2,3,6‐tricyanonaphthalene ( 5 ) with iron(II) acetate. Compound 5 is synthesized according to the route given in Scheme 1. The mononuclear bisaxial isocyanide complexes (CN) 4 ‐2,3‐NcFeL 2 7–9 with L = t BuNC, c HxNC and AdNC as well as the bridged complex [(CN) 4 ‐2,3‐NcFe(dib)] n ( 10 ) are formed as stable compounds by treating 6 with the neat ligands L. The spectroscopic properties of the complexes are described and compared with the analogous compounds (CN) 4 PcFeL 2 , 2,3‐NcFeL 2 , 1,2‐NcFeL 2 , and with PcFeL 2 . The bridged complex [(CN) 4 ‐2,3‐NcFe(dib)] n ( 10 ) exhibits only poor semiconducting properties as compared to [2,3‐NcFe(dib)] n . The oligomer 10 can be doped with iodine, and the resulting product [(CN) 4 ‐2,3‐NcFe(dib)I 1.4 ] n shows a powder conductivity s̀ RT = 2 × 10 ‐5 S/cm at room temperature." @default.
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- W1987187819 date "1992-05-01" @default.
- W1987187819 modified "2023-10-12" @default.
- W1987187819 title "(Tetracyannaphthalocyaninato)eisen(II) mit Isocyaniden als axialen Liganden" @default.
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- W1987187819 doi "https://doi.org/10.1002/cber.19921250534" @default.
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