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• W1987200150 endingPage "2720" @default.
• W1987200150 startingPage "2711" @default.
• W1987200150 abstract "The reaction of Ph3AsO with Sc(NO3)3·5H2O, Y(NO3)3·6H2O or La(NO3)3·6H2O in acetone gave [Sc(Ph3AsO)2(NO3)3], [Y(Ph3AsO)4(NO3)2]NO3, [La(Ph3AsO)4(NO3)2]NO3, and [La(Ph3AsO)3(NO3)3], whilst from ethanol solution [Sc(Ph3AsO)3(NO3)2]NO3, [Y(Ph3AsO)2(EtOH)(NO3)3] and [La(Ph3AsO)2(EtOH)(NO3)3] were produced. Similar reactions using Me3AsO produced [M(Me3AsO)6](NO3)3 (M=Sc, Y or La) and [La(Me3AsO)2(H2O)(NO3)3]. All complexes were characterised by analysis, IR and 1H, 45Sc or 89Y NMR spectroscopy, and conductance measurements. The solution speciation and interconversions of the Sc and Y complexes have been probed by 45Sc and 89Y NMR spectroscopy. X-Ray crystal structures are reported for the 6-coordinate [M(Me3AsO)6](NO3)3 (M=Sc or Y), seven-coordinate [Sc(Ph3AsO)3(NO3)2]NO3, eight-coordinate [M″(Ph3AsO)4(NO3)2]NO3 (M″=Y or La), and nine-coordinate [La(Ph3AsO)2(EtOH)(NO3)3]." @default.
• W1987200150 created "2016-06-24" @default.
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• W1987200150 date "2001-09-01" @default.
• W1987200150 modified "2023-10-04" @default.
• W1987200150 title "Scandium, yttrium and lanthanum nitrate complexes of tertiary arsine oxides: synthesis and multinuclear spectroscopic studies. X-ray structures of [M(Me3AsO)6](NO3)3 (M=Sc or Y), [Sc(Ph3AsO)3(NO3)2]NO3, [M″(Ph3AsO)4(NO3)2]NO3 (M″=Y or La) and [La(Ph3AsO)2(EtOH)(NO3)3]" @default.
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• W1987200150 doi "https://doi.org/10.1016/s0277-5387(01)00889-0" @default.
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