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- W1987603170 abstract "Activation of N-terminal resin-bound amino acids as aldimines, followed by alkylation with α,ω-dihaloalkanes, provides key intermediates for the solid-phase preparation of racemic α-substituted proline ring homologues bearing amino acid side chains. Two intramolecular displacement strategies, one involving an amine nucleophile, the other an amide nucleophile, were used to convert the intermediate ω-chloro or ω-bromo derivatives to the desired cyclic products. Using one of these routes and a fully automated synthesizer, a 48-membered library of α-substituted prolines was prepared in a combinatorial fashion." @default.
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- W1987603170 date "2003-08-16" @default.
- W1987603170 modified "2023-10-16" @default.
- W1987603170 title "The Manual and Automated Solid-Phase Synthesis of α-Substituted Prolines and Homologues" @default.
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- W1987603170 doi "https://doi.org/10.1021/cc030037q" @default.
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