FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W1987712894> ?p ?o ?g. }

• W1987712894 endingPage "211" @default.
• W1987712894 startingPage "204" @default.
• W1987712894 abstract "A new, simple, rapid and fully validated method based on gas chromatography coupled with Electron capture and ion trap mass spectrometry detectors (GC-ECD and GC-IT/MS) is presented for quantitative analysis of acrylamide contaminant in conventional cereal-based foods and potato chips. Before analysis acrylamide was efficiently derivatized with trifluoroacetic anhydride, the effects of temperature, reaction time and catalyst on the acylation reaction were evaluated. Chromatographic analysis was performed on SE-54 capillary column; good retention and peak response of the acrylamide derivative achieved under the optimal conditions. The analytical method has been fully validated by assessment of the following parameters: LODs and LOQs (1 and 25ngg(-1) by GC-ECD and 2 and 36ngg(-1) by GC-IT/MS, with a Relative Standard Deviations <4 and <6, respectively), linearity (R(2) above 0.981 in the range 0.005-50μgg(-1)) and extraction recovery (ranging between 91% and 99%, RSD below 4.0, for acrylamide spiked at levels of 1, 20, 50 and 100ngg(-1)). Furthermore, the method proposed requires no clean-up step of the acrylamide derivative to be performed prior to injection. The developed method has been successfully applied to determine acrylamide in different commercial cereal-based foods (including French fries and potato chips)." @default.
• W1987712894 created "2016-06-24" @default.
• W1987712894 creator A5025749997 @default.
• W1987712894 creator A5063744289 @default.
• W1987712894 creator A5082093604 @default.
• W1987712894 creator A5085094810 @default.
• W1987712894 creator A5085126436 @default.
• W1987712894 date "2014-03-01" @default.
• W1987712894 modified "2023-10-16" @default.
• W1987712894 title "Rapid and simple determination of acrylamide in conventional cereal-based foods and potato chips through conversion to 3-[bis(trifluoroethanoyl)amino]-3-oxopropyl trifluoroacetate by gas chromatography coupled with electron capture and ion trap mass spectrometry detectors" @default.
• W1987712894 cites W1968503158 @default.
• W1987712894 cites W1968952332 @default.
• W1987712894 cites W1975095456 @default.
• W1987712894 cites W1992161187 @default.
• W1987712894 cites W1995562090 @default.
• W1987712894 cites W2006291398 @default.
• W1987712894 cites W2015218876 @default.
• W1987712894 cites W2020355413 @default.
• W1987712894 cites W2024805816 @default.
• W1987712894 cites W2038215338 @default.
• W1987712894 cites W2044571716 @default.
• W1987712894 cites W2060304320 @default.
• W1987712894 cites W2061179224 @default.
• W1987712894 cites W2064542135 @default.
• W1987712894 cites W2068617032 @default.
• W1987712894 cites W2069811664 @default.
• W1987712894 cites W2072711409 @default.
• W1987712894 cites W2077040857 @default.
• W1987712894 cites W2079472633 @default.
• W1987712894 cites W2086316968 @default.
• W1987712894 cites W2098190319 @default.
• W1987712894 cites W2142515191 @default.
• W1987712894 doi "https://doi.org/10.1016/j.foodchem.2013.09.050" @default.
• W1987712894 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/24176333" @default.
• W1987712894 hasPublicationYear "2014" @default.
• W1987712894 type Work @default.
• W1987712894 sameAs 1987712894 @default.
• W1987712894 citedByCount "44" @default.
• W1987712894 countsByYear W19877128942012 @default.
• W1987712894 countsByYear W19877128942014 @default.
• W1987712894 countsByYear W19877128942015 @default.
• W1987712894 countsByYear W19877128942016 @default.
• W1987712894 countsByYear W19877128942017 @default.
• W1987712894 countsByYear W19877128942018 @default.
• W1987712894 countsByYear W19877128942019 @default.
• W1987712894 countsByYear W19877128942020 @default.
• W1987712894 countsByYear W19877128942021 @default.
• W1987712894 countsByYear W19877128942022 @default.
• W1987712894 countsByYear W19877128942023 @default.
• W1987712894 crossrefType "journal-article" @default.
• W1987712894 hasAuthorship W1987712894A5025749997 @default.
• W1987712894 hasAuthorship W1987712894A5063744289 @default.
• W1987712894 hasAuthorship W1987712894A5082093604 @default.
• W1987712894 hasAuthorship W1987712894A5085094810 @default.
• W1987712894 hasAuthorship W1987712894A5085126436 @default.
• W1987712894 hasConcept C106159729 @default.
• W1987712894 hasConcept C111771559 @default.
• W1987712894 hasConcept C119128265 @default.
• W1987712894 hasConcept C123460561 @default.
• W1987712894 hasConcept C15920480 @default.
• W1987712894 hasConcept C162324750 @default.
• W1987712894 hasConcept C162356407 @default.
• W1987712894 hasConcept C178790620 @default.
• W1987712894 hasConcept C185592680 @default.
• W1987712894 hasConcept C205345274 @default.
• W1987712894 hasConcept C2779402116 @default.
• W1987712894 hasConcept C2780112151 @default.
• W1987712894 hasConcept C2781143453 @default.
• W1987712894 hasConcept C43617362 @default.
• W1987712894 hasConcept C4725764 @default.
• W1987712894 hasConcept C521977710 @default.
• W1987712894 hasConceptScore W1987712894C106159729 @default.
• W1987712894 hasConceptScore W1987712894C111771559 @default.
• W1987712894 hasConceptScore W1987712894C119128265 @default.
• W1987712894 hasConceptScore W1987712894C123460561 @default.
• W1987712894 hasConceptScore W1987712894C15920480 @default.
• W1987712894 hasConceptScore W1987712894C162324750 @default.
• W1987712894 hasConceptScore W1987712894C162356407 @default.
• W1987712894 hasConceptScore W1987712894C178790620 @default.
• W1987712894 hasConceptScore W1987712894C185592680 @default.
• W1987712894 hasConceptScore W1987712894C205345274 @default.
• W1987712894 hasConceptScore W1987712894C2779402116 @default.
• W1987712894 hasConceptScore W1987712894C2780112151 @default.
• W1987712894 hasConceptScore W1987712894C2781143453 @default.
• W1987712894 hasConceptScore W1987712894C43617362 @default.
• W1987712894 hasConceptScore W1987712894C4725764 @default.
• W1987712894 hasConceptScore W1987712894C521977710 @default.
• W1987712894 hasFunder F4320324633 @default.
• W1987712894 hasLocation W19877128941 @default.
• W1987712894 hasLocation W19877128942 @default.
• W1987712894 hasOpenAccess W1987712894 @default.
• W1987712894 hasPrimaryLocation W19877128941 @default.
• W1987712894 hasRelatedWork W2033335551 @default.
• W1987712894 hasRelatedWork W2107172911 @default.
• W1987712894 hasRelatedWork W2115421738 @default.
• W1987712894 hasRelatedWork W2118427679 @default.
• W1987712894 hasRelatedWork W2169905038 @default.
• W1987712894 hasRelatedWork W2336968138 @default.

• next