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• W1987816214 abstract "A simple and general method for the synthesis of highly substituted α-tropolone ethers that allows rapid access to the bis(tropolone) core of the antiproliferative metabolites (−)-gukulenins A and F (3, 4) is described. The reaction proceeds by thermolytic opening of gem-dibromobicyclo[4.1.0]heptane intermediates, which are readily accessed from simple starting materials. Mechanistic studies suggest the reaction proceeds via an autocatalytic process mediated by methyl hypobromite. This synthetic sequence allows access to a broad array of highly substituted α-tropolones." @default.
• W1987816214 created "2016-06-24" @default.
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• W1987816214 date "2015-04-03" @default.
• W1987816214 modified "2023-10-05" @default.
• W1987816214 title "The Discovery of a Novel Route to Highly Substituted α-Tropolones Enables Expedient Entry to the Core of the Gukulenins" @default.
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• W1987816214 doi "https://doi.org/10.1021/acs.orglett.5b00841" @default.
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