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- W1987884143 abstract "Abstract Silica-functionalized CuI has been reported as an efficient and selective catalyst for the selective mono-N- and N,N-dibenzylation, allylation, and alkylation of primary amines with benzylic, allylic, and alkyl halides using NaOH as base in aqueous medium. By changing the reaction temperature, mono- or di-benzylation, allylation, or alkylation could be achieved in good yield and selectivity. Secondary amines have also been benzylated, allylated, and alkylated under similar conditions. SiO2-CuI has been characterized by Fourier transform–infrared, atomic absorption spectrometry, thermalgravimetric analysis, X-ray diffraction, scanning electron microscopy, and transmission electron microscopy, and found to be highly selective and recyclable under the reaction conditions. [Supplementary materials are available for this article. Go to the publisher's online edition of Synthetic Communications® for the following free supplemental resource(s): Full experimental and spectral details.]" @default.
- W1987884143 created "2016-06-24" @default.
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- W1987884143 date "2013-12-27" @default.
- W1987884143 modified "2023-09-24" @default.
- W1987884143 title "Silica-Functionalized CuI: An Efficient and Selective Catalyst for <i>N</i>-Benzylation, Allylation, and Alkylation of Primary and Secondary Amines in Water" @default.
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- W1987884143 doi "https://doi.org/10.1080/00397911.2013.828077" @default.
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