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• W1988156714 abstract "Metallated dihydropyran 9 and the dihydropyranone 10 previously used in a synthesis of the insect toxin pederin were adapted to the synthesis of 18-O-methyl mycalamide B, the most potent derivative of the anti-tumour agents isolated from a sponge. Key steps in the synthesis include the oxidation of enol silane 11 from the more hindered face using dimethyldioxirane to introduce the hydroxy group at C-12 and the acylation of 6-lithio-3,4-dihydro-2H-pyran 9 with oxalamide 8 to forge the N-(1-alkoxy-1-alkyl)amide bridge. Biological tests in human tumour cell lines confirm the potent anti-proliferative effect of 18-O-methyl mycalamide B in pM concentrations." @default.
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• W1988156714 date "1996-01-01" @default.
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• W1988156714 title "A synthesis of 18-O-methyl mycalamide B" @default.
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• W1988156714 doi "https://doi.org/10.1039/p19960001797" @default.
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