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• W1988197595 abstract "The preparation of Mg(2-Me-1,2-C2B10H10)2·2C4H8O2 from the carboranyl Grignard reagent RMgBr (R = the methyl-ortho-carboranyl residue, 2-Me-1,2-C2B10H10) by a dioxane-induced disproportionation reaction is described. An X-ray crystallographic study of the product has revealed a monomeric molecular structure R2MgL2 (L = 1,4-dioxane, C4H8O2) in which the carboranyl groups and dioxane ligands provide the central magnesium atom with a distorted tetrahedral coordination sphere of two carbon and two oxygen atoms, with bond lengths MgC 2.156(5) Å, MgO 2.038(8) Å and bond angles CMgC 123.5(4)°, OMgO 99.5(5)°, distortions from regular tetrahedral angles attributable to the relative bulk of the carboranyl ligands." @default.
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• W1988197595 date "1987-05-01" @default.
• W1988197595 modified "2023-10-14" @default.
• W1988197595 title "Preparation and crystal structure of the dicarboranyl-magnesium bis(dioxane) adduct Mg(2-Me-1,2-C2B10H10)2·2C4H8O2" @default.
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• W1988197595 doi "https://doi.org/10.1016/0022-328x(87)80386-8" @default.
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