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• W1988333374 endingPage "1682" @default.
• W1988333374 startingPage "1677" @default.
• W1988333374 abstract "Treatment of [Et4N][(Me2Tp)W(CO)3] (Me2Tp = HB(3,5-dimethylpyrazol-1-yl)3) with S8 in DMF at room temperature afforded a tris(sulfido) complex [Et4N][(Me2Tp)WS3] (1a), while that of [Et4N][TpW(CO)3] (Tp = HB(pyrazol-1-yl)3) in MeCN resulted in the formation of [Et4N][TpWS3] (1b) along with [Et4N]2[[WO(S2)2]2(mu-S)] (6) as a byproduct. Under similar conditions, [Et4N][(Me2Tp)Mo(CO)3] gave a mixture of a sulfido-tetrasulfido complex [Et4N][(Me2Tp)MoS(S4)] (2a) and its monooxo analogue [Et4N][(Me2Tp)MoO(S4)], although a sulfido-tetrasulfido complex [Et4N][TpMoS(S4)] (2b) was exclusively obtained from [Et4N][TpMo(CO)3]. The reaction of 1a with [PtCl2(cod)] (cod = 1,5-cyclooctadiene) in MeCN at room temperature led to the formation of a sulfido-bridged mixed-metal complex [Et4N][(Me2Tp)WS(mu-S)2PtCl2] (10). The structures of new complexes have been determined in detail by the X-ray analyses for 1a.MeCN, 1b, 2a, 2b, 6, and 10." @default.
• W1988333374 created "2016-06-24" @default.
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• W1988333374 date "2001-03-01" @default.
• W1988333374 modified "2023-09-26" @default.
• W1988333374 title "Preparation of Mononuclear Tungsten Tris(sulfido) and Molybdenum Sulfido−Tetrasulfido Complexes with Hydridotris(pyrazolyl)borate Coligand and Conversion of the Former into Sulfido-Bridged Bimetallic Complex Having Pt(μ-S)₂WS Core" @default.
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• W1988333374 doi "https://doi.org/10.1021/ic0008823" @default.
• W1988333374 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/11261979" @default.
• W1988333374 hasPublicationYear "2001" @default.
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