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• W1988341367 endingPage "266" @default.
• W1988341367 startingPage "255" @default.
• W1988341367 abstract "Dehydration of Cu(II)-exchanged ZSM-5 and rehydration have been studied by electron spin resonance (ESR) and electron spin echo modulation (ESEM). The ESEM results indicate that Cu(II) is present in hydrated Cu-ZSM-5 as paramagnetic Cu(II)–OH− with five coordinated water molecules. Upon thermal dehydration, the ESR intensity decreases by about 85%, and it is suggested that Cu(I) and Cu(II)–O− are formed among other possible species. The remaining isolated paramagnetic Cu(II) is identified by ESR as three different species: I, II and III with g‖ values of 2.314, 2.301 and 2.272, respectively. After NO adsorption onto dehydrated Cu-ZSM-5, NO interactions with Cu(I), Cu(II)–O− and Cu(II) have been studied by ESR and fourier transform infrared spectroscopy. It is suggested that Cu(II)–O− interacts with NO to form Cu(I)–(NO2) and that further interaction with NO yields Cu(II)–(NO2)(NO). Cu(I) is also suggested to react with one or two NO to form Cu(I)–NO and Cu(I)–(NO)2 of which the latter further transforms to Cu(II)–(N2O)O−. Among the three paramagnetic Cu(II) ions, only species III reacts with NO to form Cu(II)–NO; the other two Cu(II) species are inactive toward NO adsorption. A schematic mechanism based on these and earlier results is proposed for NO adsorption, interaction and transformation over Cu-ZSM-5." @default.
• W1988341367 created "2016-06-24" @default.
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• W1988341367 date "2000-08-01" @default.
• W1988341367 modified "2023-09-26" @default.
• W1988341367 title "Reaction of NO with copper ions in Cu(II)-exchanged ZSM-5 zeolite: electron spin resonance, electron spin echo modulation and Fourier transform infrared spectroscopy" @default.
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• W1988341367 doi "https://doi.org/10.1016/s1387-1811(00)00145-1" @default.
• W1988341367 hasPublicationYear "2000" @default.
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