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• W1988597788 abstract "A detailed characterization of two samples synthesized at $13phantom{rule{0.3em}{0ex}}mathrm{GPa}$ and $830phantom{rule{0.3em}{0ex}}mathrm{K}$ with heating times of $20phantom{rule{0.3em}{0ex}}mathrm{min}$ and $1phantom{rule{0.3em}{0ex}}mathrm{h}$, respectively, was performed using x-ray diffraction (XRD), Raman spectroscopy, and high-resolution transmission electron microscopy (HRTEM). The sample heated for $20phantom{rule{0.3em}{0ex}}mathrm{min}$ was amorphous and exhibited a high hardness of $45phantom{rule{0.3em}{0ex}}mathrm{GPa}$, while the second sample appeared to be softer and crystalline. A slightly distorted fcc cubic packing was found by XRD and HRTEM. Both samples are proved to consist of unbroken ${mathrm{C}}_{60}$ molecules. The crystalline sample was also studied by in situ XRD during compression up to $26phantom{rule{0.3em}{0ex}}mathrm{GPa}$ using synchrotron radiation. The bulk modulus value of $217phantom{rule{0.3em}{0ex}}mathrm{GPa}$ obtained from compression experiments is in good agreement with the measured hardness of the sample $(37phantom{rule{0.3em}{0ex}}mathrm{GPa})$. The Raman spectroscopy shows an unusual combination of features: some additional peaks compared to untreated ${mathrm{C}}_{60}$ and no shift for the ${A}_{g}(2)$ mode." @default.
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• W1988597788 date "2005-03-24" @default.
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• W1988597788 title "Structural characterization of the hard fullerite phase obtained at<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML display=inline><mml:mrow><mml:mn>13</mml:mn><mml:mspace width=0.3em /><mml:mi>GPa</mml:mi></mml:mrow></mml:math>and<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML display=inline><mml:mrow><mml:mn>830</mml:mn><mml:mspace width=0.3em /><mml:mi mathvariant=normal>K</mml:mi></mml:mrow></mml:math>" @default.
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• W1988597788 doi "https://doi.org/10.1103/physrevb.71.115424" @default.
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