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- W1988598668 abstract "Tetragonal neodymium disilicate (i.e., Nd2Si2O7) powder was synthesized in the absence and presence of 5 wt% lithium chloride (i.e., LiCl) as a mineralizer by sol–gel method and subsequent thermal treatment process. The effect of LiCl on the crystallization process of the synthesized xerogel was investigated by differential thermal analysis (DTA), X-ray diffraction (XRD) and scanning electron microscopy (SEM), respectively. The crystallization kinetic was analyzed at different heating rates (i.e., 2, 5, 10 and 20 K/min) by a non-isothermal differential thermal analysis method. The activation energies of the tetragonal Nd2Si2O7 crystallization calculated by the Kissinger and the Ligero methods are 673 kJ/mol for the xerogel without LiCl and 586 kJ/mol for the xerogel with 5 wt% LiCl. In addition, the crystallization mechanism was also discussed, indicating that the crystallization mechanism of the tetragonal Nd2Si2O7 changes from bulk and homogeneous to two-dimension crystallization in the presence of 5 wt% LiCl." @default.
- W1988598668 created "2016-06-24" @default.
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- W1988598668 date "2014-11-01" @default.
- W1988598668 modified "2023-09-27" @default.
- W1988598668 title "Effect of lithium chloride on crystallization process of neodymium disilicate" @default.
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- W1988598668 doi "https://doi.org/10.1016/j.ceramint.2014.06.025" @default.
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