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• W1988991292 endingPage "2436" @default.
• W1988991292 startingPage "2428" @default.
• W1988991292 abstract "A heteropolyoxotungstate, [Cu(en)2]2H8[Gd(PW11O39)2] · (H2en)0.5 · 3H2O (1), has been hydrothermally synthesized and characterized by IR, XPS, TGA and single-crystal X-ray diffraction. Compound 1 crystallizes in the triclinic system, space group P 1, with a = 12.651(2) Å3, b = 20.559(3) Å3, c = 21.729(3) Å3, α = 71.379(2), β = 82.829(2), γ = 75.532(2)°, V = 5179.5(14) Å3, Z = 2, R 1 = 0.0702 and ωR 2 = 0.1479. The heteropolyanion is composed of two monovacant [α-PW11O39]7− Keggin moieties linked via a Gd atom leading to a sandwich-type structure. The Gd center is in a distorted square antiprismatic coordination environment with eight oxygen atoms, four from each of the two [α-PW11O39]7−moieties." @default.
• W1988991292 created "2016-06-24" @default.
• W1988991292 creator A5055332524 @default.
• W1988991292 creator A5064838211 @default.
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• W1988991292 date "2008-08-10" @default.
• W1988991292 modified "2023-10-10" @default.
• W1988991292 title "Hydrothermal synthesis and crystal structure of a heteropolyoxotungstate formed by sandwich-type heteropolyanion [Gd(PW11O39)2]11− and reduced [Cu(en)2] + cations" @default.
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• W1988991292 doi "https://doi.org/10.1080/00958970801914793" @default.
• W1988991292 hasPublicationYear "2008" @default.
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