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- W1989031273 abstract "A surface hydroperoxide intermediate has been detected upon oxidation of water at an Ir oxide nanocluster catalyst system under pulsed excitation of a [Ru(bpy)3]2+ visible light sensitizer by recording of the OO vibrational mode at 830 cm–1. Rapid-scan FT-IR spectroscopy of colloidal H2O, D2O, and D218O solutions in the attenuated total reflection mode allowed spectral assignment of IrOOH on the basis of an observed D shift of 30 cm–1, and 18O shifts of 24 cm–1 (16O18O) and 46 cm–1 (18O18O). The laser pulse response of the infrared band is consistent with the kinetic relevancy of the intermediate. This is the first observation of a surface intermediate of oxygen evolution at an Ir oxide multielectron catalyst." @default.
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- W1989031273 date "2011-08-01" @default.
- W1989031273 modified "2023-10-11" @default.
- W1989031273 title "Direct Observation of a Hydroperoxide Surface Intermediate upon Visible Light-Driven Water Oxidation at an Ir Oxide Nanocluster Catalyst by Rapid-Scan FT-IR Spectroscopy" @default.
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- W1989031273 doi "https://doi.org/10.1021/ja205300a" @default.
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