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- W1989059101 abstract "The reactions of the dimers [Ru(η6-arene)Cl2]2] (arene=C6H5Me, p-MeC6H4i-Pr or C6Me6) with (n-Bu4N)2[Mo2O7] have been investigated in methanol or acetonitrile, in some cases in the presence of MeC(CH2OH)3. A series of complexes with various nuclearities, [{Ru(η6-arene)}Mo2O4{MeC(CH2O)3}2] and [{Ru(η6-arene)}2Mo2O6(OMe)4] (arene=p-MeC6H4i-Pr), (n-Bu4N)2[{Ru(η6-arene)}2Mo6O20(OMe)2] (arene=C6H5Me or C6Me6) and (n-Bu4N)2[{Ru(η6-arene)}2Mo6O18{MeC(CH2O)3}2] (arene=C6Me6), has been obtained. The crystal structures of these compounds have been determined by X-ray crystallography. The clusters [{Ru(η6-arene)}Mo2O4{MeC(CH2O)3}2], [{Ru(η6-arene)}2Mo2O6(OMe)4], [{Ru(η6-arene)}2Mo6O20(OMe)2]2− and [{Ru(η6-arene)}2Mo6O18{MeC(CH2O)3}2]2− were derived from known oxoalkoxopolymolybdates, [Mo3O6(OMe){MeC(CH2O)3}2]−, [Mo4O10(OMe)6]2−, [Mo8O24(OMe)4]4− and [Mo8O20(OMe)4{MeC(CH2O)3}2]2−, respectively, through the formal replacement of d0-fac-{MoO2(OMe)}+ groups by topologically equivalent {Ru(η6-arene)}2+ units and, for the octanuclear trisalkoxo derivatives, by further substitution of two oxo ligands for the two remaining methoxo ligands." @default.
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- W1989059101 date "2003-08-01" @default.
- W1989059101 modified "2023-10-10" @default.
- W1989059101 title "Organometallic polyoxometalates: synthesis and structural analysis of (η6-arene) ruthenium-containing polyoxomolybdates" @default.
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- W1989059101 doi "https://doi.org/10.1016/s0022-2860(03)00356-9" @default.
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