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- W1989616964 abstract "Abstract The compound Cu(p-OHC 6 H 4 COO) 2 (DENC) 2 (DENC = N,N′-diethylnicotinamide) crystallizes in the orthorhombic system, space group Pbca (No. 61), with unit cell parameters a = 44.966(1) Å, b = 16.267(1) Å, c = 14.0147(3) Å, and Z = 12. The final R value for 5528 independent reflexions is equal to 0.054. Its structure consists of centrosymmetric [Cu(p-OHC 6 H 4 COO) 2 (DENC) 2 ] units and infinite polymer chains, interconnected by hydrogen bonds. Within a monomeric unit, the Cu atom is pseudooctahedrally trans-coordinated by four carboxylic O atoms of two p-hydroxobenzoate ligands [Cu–O bond distances being 1.923(4) Å (2×) and 2.582(3) Å (2×), and by two N atoms from two DENC ligands [Cu–N bond distances are 2.050(3) Å (2×)]. Each Cu aton in the chain is hexacoordinated by three carboxylic O atoms from the monodentate and tridentate p-hydroxobenzoates [Cu–O bond distances are 1.929(4) Å, 1.962(4) Å and 2.652(3) Å], by two N atoms from two DENC ligands [Cu–N bond distances are 2.019(3) Å and 2.025(3) Å] and one hydroxyl O atom of further tridentate p-hydroxobenzoate [Cu–O bond distance is 2.378(3) Å]." @default.
- W1989616964 created "2016-06-24" @default.
- W1989616964 date "1994-03-01" @default.
- W1989616964 modified "2023-09-23" @default.
- W1989616964 title "Structure of bis (p-hydroxobenzoato)di(N,N′-diethylnicotinamide)-copper(II)" @default.
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- W1989616964 doi "https://doi.org/10.1524/zkri.1994.209.3.267" @default.
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