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• W1989965379 abstract "Abstract The microstructure of a nanocrystalline Pd sample prepared by inert gas condensation was studied by small-angle neutron scattering. To increase information, the contrast of the sample was additionally varied by doping it with H and D ( c H =3.2 at%, c D =3.5 at%). We modeled the measured intensity by a Porod contribution caused by large heterogenities (pores) and a second contribution caused by a logarithmic normal distribution of spherical grains surrounded by shells of reduced Pd density describing the grain boundaries. This model yields a volume-weighted mean grain radius of 10 nm and a grain boundary thickness of approximately 0.8 nm. The contrast variation due to doping with H and D indicated that H and D were mainly located in grain boundaries." @default.
• W1989965379 created "2016-06-24" @default.
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• W1989965379 date "2000-03-01" @default.
• W1989965379 modified "2023-10-02" @default.
• W1989965379 title "Small-angle neutron scattering on hydrogen- and deuterium-doped nanocrystalline palladium" @default.
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• W1989965379 doi "https://doi.org/10.1016/s0921-4526(99)01631-2" @default.
• W1989965379 hasPublicationYear "2000" @default.
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