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- W1989980023 abstract "Reaction of Nb(OEt)5 with 2-mercapto-4-methylphenol (mmpH2) in the presence of triethylamine gave the mononuclear tris complex (Et3NH)[Nb(mmp)3] which was structurally characterized. The coordination geometry around the niobium is between octahedral and trigonal prismatic, with a twist angle of 41.5°. The mercaptophenolate ligands are arranged around the metal in a “propeller” fashion. (Et3NH)[Nb(mmp)3] was characterized by IR, 1H NMR and UV-vis spectroscopies, and cyclic voltammetry. A reversible reduction wave found at −1.03 V is for reduction to the NbIV complex." @default.
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- W1989980023 date "1997-01-01" @default.
- W1989980023 modified "2023-10-14" @default.
- W1989980023 title "A niobium(V) complex with mixed O,S-donor ligands. Synthesis, structure and properties of the anion tris(2-mercapto-4-methylphenolato)niobate(V)" @default.
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- W1989980023 doi "https://doi.org/10.1016/s0277-5387(96)00451-2" @default.
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