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- W1990224503 abstract "L-idaro-1,4-lactone was synthesized by two different, published methods: (1) epimerization of monopotassium D-glucarate by refluxing in aqueous barium hydroxide, and (2) oxidation of L-iditol by heating in dilute nitric acid. The lactone, formed by heat dehydration from aqueous solution at low pH, was purified by paper chromatography, and quantitated by gas-liquid chromatography using inositol as the internal standard. The monolactone inhibited human, seminal-fluid alpha-L-idosiduronase activity, with either phenyl or 4-methylumbelliferyl alpha-L-idosiduronic acid as the substrate, to the same degree as D-glucaro-1,4-lactone inhibits alpha-D-glucosiduronase." @default.
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- W1990224503 date "1982-01-01" @default.
- W1990224503 modified "2023-10-14" @default.
- W1990224503 title "Synthesis of l-idaro-1,4-lactone, an inhibitor of α-l-idosiduronase" @default.
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- W1990224503 doi "https://doi.org/10.1016/s0008-6215(00)80972-6" @default.
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