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• W1990264902 abstract "Abstract Ultrafine (Ti, W, Mo, V)(C, N)–Ni composite powders with globular-like particles of ∼50–300 nm were synthesized at static nitrogen pressure from oxides by a simple and cost-effective route which combines traditional low-energy milling plus carbothermal reduction–nitridation (CRN) techniques. Reaction path of the (Ti, W, Mo, V)(C, N)–Ni system was discussed by X-ray diffraction (XRD) and thermogravimetry–differential scanning calorimetry (TG–DSC), and microstructure of the milled powders and final products was studied by scanning electron microscopy (SEM) and transmission electron microscope (TEM), respectively. The results show that CRN reaction has been enhanced by nano-TiO2 and nano-carbon powders. Thus, the preparation of (Ti, 15W, 5Mo, 0.2V)(C, N)–20Ni is at only 1300 °C for 1 h. During synthesizing reaction, Ni solid solution phase forms at about 700 °C and reduction–carbonization of WO2 and MoO2 occurs below 900 °C. The reactions of TiO2 → Ti3O5, Ti3O5 → Ti(C, O) and Ti(C, O) → Ti(C, N) take place at about 930 °C, 1203 °C and 1244 °C, respectively." @default.
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• W1990264902 date "2009-11-01" @default.
• W1990264902 modified "2023-09-27" @default.
• W1990264902 title "Synthesis of ultrafine (Ti, W, Mo, V)(C, N)–Ni composite powders by low-energy milling and subsequent carbothermal reduction–nitridation reaction" @default.
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• W1990264902 doi "https://doi.org/10.1016/j.jallcom.2009.07.088" @default.
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