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• W1990325030 endingPage "328" @default.
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• W1990325030 abstract "The first iridium(I) complex containing siloxyl and N-heterocyclic carbene ligand such as [Ir(cod)(IMes)(OSiMe3)] (1) and [Ir(CO)2(IMes)(OSiMe3)] (3) have been synthesized and their structures solved by spectroscopy and X-ray methods as well as catalytic properties in selected hydrogenation reactions have been presented in comparison to their chloride analogues, i.e. [Ir(Cl)(cod)(IMes)] (2) and [Ir(Cl)(CO)2(IMes)] (4). The attempts at synthesis of iridium(I) complex with tert-butoxyl ligand has failed as leading instead to the iridium hydroxide complex [Ir(cod)(OH)(IMes)] (5) whose X-ray structure has also been solved. All complexes (1)–(5) show square planar geometry typical of the four-coordinated iridium complexes. Catalytic activity of complexes 1 and 2 was tested in transfer hydrogenation of acetophenone and hydrogenation of olefins." @default.
• W1990325030 created "2016-06-24" @default.
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• W1990325030 date "2008-01-01" @default.
• W1990325030 modified "2023-10-04" @default.
• W1990325030 title "Synthesis, structure and catalytic activity of the first iridium(I) siloxide versus chloride complexes with 1,3-mesitylimidazolin-2-ylidene ligand" @default.
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• W1990325030 doi "https://doi.org/10.1016/j.jorganchem.2007.11.013" @default.
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