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- W1990362980 abstract "Photoreduction of CO 2 using p-terphenyl as a photosensitizer and a tertiary amine as a sacrificial electron donor is efficiently catalyzed by cobalt macrocycles in methanolic acetonitrile solutions. Studies of the mechanism of CO 2 reduction in the catalytic system using Co II HMD 2+ (HMD = 5,7,7, 12, 14,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene) have been carried out using continuous and flash photolysis techniques. The transient spectra reveal the formation of p-terphenyl radical anion, the Co I HMD + complex, the 5-coordinate [Co I HMD-CO 2 ] + complex, and the six coordinate [S-Co III HMD-(CO 2 2− )] + complex (S = solvent) in the catalytic system. The importance of changes in the Co II/I reduction potential and the geometry around the Co center was studied by the use of several different complexes" @default.
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- W1990362980 date "1995-06-01" @default.
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- W1990362980 title "Mechanistic and kinetic studies of cobalt macrocycles in a photochemical CO2 reduction system" @default.
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- W1990362980 doi "https://doi.org/10.1016/0196-8904(95)00094-t" @default.
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