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- W1990603406 abstract "A new application of electron paramagnetic resonance (EPR) spin trapping is described using the nitromethane aci anion (CH2NO2-) spin trapping technique for quantitative measurement of nitrogen dioxide radicals (•NO2) and nitrite ions (NO2-) in strong alkaline aqueous solution. The relative concentration of a spin adduct radical, dinitromethyl dianion radical [-O2N−CHNO2•-] (I), produced by ultraviolet photolysis, is shown to be proportional to the concentration of NO2- dissolved in alkaline solution. This method is applied to estimate the •NO2 concentrations produced by decomposition of two energetic nitramine compounds: cyclotrimethylenetrinitramine, C6H6N6O6 (RDX), and ammonium dinitramide, NH4+N(NO2)2- (ADN), by using calibration plots of the spin concentration of I versus time of photolysis. Calibrations were prepared using sodium nitrite (NaNO2) or ammonium nitrate (NH4NO3) which behave similarly to the energetic compounds with respect to formation of I." @default.
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- W1990603406 date "1997-03-01" @default.
- W1990603406 modified "2023-09-28" @default.
- W1990603406 title "Quantitative EPR Spin Trapping. 1. Nitrogen Dioxide Radicals and Nitrite Ions from Energetic Materials in Alkaline Aqueous Solution" @default.
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- W1990603406 doi "https://doi.org/10.1021/jp961578r" @default.
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