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- W1990907393 abstract "Abstract erythro -Hydroxyasparagine ( e HyAsn, 1 ) occurs in a number of naturally occurring peptides and proteins. Previous syntheses have relied on enzyme-catalyzed reactions to produce relevant, optically active intermediates. We report herein a completely chemical synthesis that intercepts Boger’s synthesis of the diastereomer ( t HyAsn, 4 ), utilizing a Sharpless asymmetric aminohydroxylation reaction to introduce the two stereocenters. Boc-HyAsn(OTBS)-OH ( 10 ) was coupled effectively with phenylalanine methyl ester using EDC/HOBt." @default.
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- W1990907393 date "2009-03-01" @default.
- W1990907393 modified "2023-10-09" @default.
- W1990907393 title "Asymmetric synthesis of erythro-β-hydroxyasparagine" @default.
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- W1990907393 doi "https://doi.org/10.1016/j.tetlet.2008.12.103" @default.
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