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- W1990975269 abstract "Abstract Needle-shaped crystals of Nb 7 W 10 O 47 , a member of the solid solution series Nb 8− n W 9+ n O 47 with n =1, were prepared from the binary oxides with HgCl 2 added as a mineralizer. All investigated crystals were twinned. The data set was measured on a fourling, which consists of 73% of an individual twin domain. The orthorhombic structure ( a =1225.7(2), b =3663.3(6), c =394.96(6) pm) was refined in the space group P 2 1 2 1 2 (No. 18) to a final R value of 5.11%. The composition of this crystal determined from X-ray data is Nb 6.7 W 10.3 O 47 . Nb 7 W 10 O 47 crystallizes isostructural to Nb 8 W 9 O 47 in a threefold superstructure of the tetragonal tungsten bronze type. All atomic positions are considerably shifted out of the planes (001) and (002), leading to alternating short (∼175 pm) and long (∼220 pm) metal–oxygen distances along the short crystallographic c axis. One octahedral site is exclusively occupied by W, the center of the pentagonal bipyramid preferentially by Nb." @default.
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- W1990975269 date "2000-02-01" @default.
- W1990975269 modified "2023-10-18" @default.
- W1990975269 title "Superstructure and Twinning in the Tetragonal Tungsten Bronze-Type Phase Nb7W10O47" @default.
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- W1990975269 doi "https://doi.org/10.1006/jssc.1999.8575" @default.
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