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- W1990998435 abstract "Langanite (La 3 Ga 5.5 Nb 0.5 O 14 , growth atmosphere: 99% Ar + 1% O 2 ) and kanigasite (Ca 3 NbGa 3 Si 2 O 14 , growth atmosphere: 100% Ar) crystals grown by the Czochralski technique in Ir crucibles along <0001> direction have been firstly investigated by neutron diffraction. The difference between the compositions of upper (La 2.935(2) □ 0.065 )(Ga 0.450 Nb 0.550(3) )Ga 3 (Ga 1.965(4) □ 0.035 )(O 13.90(1) □ 0.10 ) and lower (La 2.940(1) □ 0.060 )(Ga 0.590 Nb 0.410(2) )Ga 5 (O 13.82(1) □ 0.18 ) parts of orange langanite crystal was found. It was established that the colorless Ca 3 NbGa 3 Si 2 O 14 crystal grown by using the single-crystal charge has the composition (Ca 2.95 □ 0.05(1) )NbGa 3 Si 2 O 14 and is less defective in comparison to the yellow one grown by using the charge prepared by conventional solid-state reaction. For Ca 3 NbGa 3 Si 2 O 14 and La 3 Ga 5.5 Nb 0.5 O 14 crystals the possibility of microtwin formation (two unit cells connected by the translation: 1/2 z ) was revealed for the first time. It was found that the difference between the color of crystals is attributed to the qualitative differentiation of oxygen vacancies." @default.
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- W1990998435 date "2013-03-14" @default.
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- W1990998435 title "Growth and Neutron Diffraction Investigation of Ca3NbGa3Si2O14 and La3Ga5.5Nb0.5O14 Crystals" @default.
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- W1990998435 doi "https://doi.org/10.1155/2013/191626" @default.
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