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- W1991231161 abstract "The cystral structure of the disubstituted cluster, Ru 3 (CO) 10 (PPh 3 ) 2 , prepared from Ru 3 (CO) 12 and PPh 3 , was determined by single crystal X-ray diffraction methods. The crystals are orthorhombic, space group P 2 1 2 1 2 1 with a 14.851(2), b 17.039(3), c 34.693(5) Å, and Z = 8. The structure was refined to R 8.2% for 4616 observed reflections. The cluster consists of a triangle of Ru atoms with the PPh 3 ligands equatorially bonded to different Ru atoms and approximately trans to one of the RuRu bonds. The configuration of the four carbonyls on the unique ruthernium is substantially twisted from that found for the Ru(CO) 4 group of Ru 3 (CO)_ 12 . This configuration allows a semibridging orientation of several carbonyls, attributed to both the steric and electronic effects of the PPh 3 substitution." @default.
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- W1991231161 date "1988-05-01" @default.
- W1991231161 modified "2023-09-23" @default.
- W1991231161 title "The crystal structure of bis(triphenylphosphine)decarcarbonyl-triruthenium, Ru3(CO)10(PPh3)2. An example of unsymmetrical semibridging carbonyls in a substituted cluster" @default.
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- W1991231161 doi "https://doi.org/10.1016/0022-328x(88)80120-7" @default.
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