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- W1991352685 abstract "A procedure for the determination of nitro-substiruted polynuclear aromatic hydrocarbons (nitro-PAH) on crude air-particulate and soil extracts is introduced. Elimination of purification and fractionation procedures was made possible by the use of both a selective ionization method, such as electron-capture chemical ionization, and a specific fragmentation process, in an experiment of tandem mass spectrometry (gas chromatography—electron capture tandem mass spectrometry). Different mass spectrometric procedures were compared. The best performance was observed when the nitro-PAH molecular ions [M]− were mass-selected by the first analyzer under multiple reaction monitoring conditions and then fragmented to NO2− (m/z 46). Detection limits were on the order of hundreds of femtograms, as determined in extracts of real environmental samples. This corresponds approximately to 5–15 pg of nitro-PAH per cubic meter of air sampled. Calibration curves were linear over 3 orders of magnitude. Applications to contamination from motor vehicle combustion and the iron industry are briefly discussed." @default.
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- W1991352685 date "1996-12-01" @default.
- W1991352685 modified "2023-10-11" @default.
- W1991352685 title "Sub-parts-per-billion determination of nitro-substituted polynuclear aromatic hydrocarbons in airborne particulate matter and soil by electron capture-Tandem mass spectrometry" @default.
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- W1991352685 doi "https://doi.org/10.1016/s1044-0305(96)00106-7" @default.
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