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• W1991569351 abstract "A multiple flame photometric detector (mFPD) based on many flames operated in series is introduced for the detection of sulfur and phosphorus compounds. The method employs attributes of a previously developed micro counter-current flame technique to readily establish any number of very small compact flames inside a narrow quartz tube. Results show for the first time that a five flame mFPD mode can improve hydrocarbon quenching resistance nearly 20-fold relative to a single flame (i.e., conventional FPD) mode, and nearly 10-fold relative to a two flame (i.e., dual FPD) mode. Under these conditions, the five flame mFPD mode is shown to maintain about 60% of its original analyte chemiluminescence even in the presence of over 100 mL/min of methane flow into the detector. In contrast to a conventional dual FPD device, the five flame mFPD mode also provides analyte sensitivity that is similar to a conventional FPD. Of note, the mFPD yields minimum detectable limits for sulfur and phosphorus of 4 × 10−11 g S/s and 3 × 10−12 g P/s respectively. Analyte selectivity over hydrocarbons, signal reproducibility, and response equimolarity are also improved in the mFPD, making it a potentially useful detector for applications in gas chromatography." @default.
• W1991569351 created "2016-06-24" @default.
• W1991569351 creator A5007289411 @default.
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• W1991569351 date "2009-10-06" @default.
• W1991569351 modified "2023-09-25" @default.
• W1991569351 title "Quenching-Resistant Multiple Micro-Flame Photometric Detector for Gas Chromatography" @default.
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• W1991569351 doi "https://doi.org/10.1021/ac901421s" @default.
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