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- W1991578049 abstract "Abstract Reversed-phase chromatographic surfaces were prepared by reacting 1- 13 C-nonyltrichlorosilane, 12- 13 C-dodecyltrichlorosilane, 12- 13 C-dodecyldimethylchlorosilane, 12- 13 C-tridecyltrichlorosdane, and 12- 13 C-tridecyldimethylchlorosilane with porous silica. For each of these labeled materials 13 C spin-lattice relaxation times were measured as a function of temperature under both dry and solvated conditions. Activation energies are nearly constant irrespective of the position of the carbon atom in the chain for the dry state materials. However, in the presence of solvent, activation energy depends on the position of carbon in the chain and the contact solvent. These results reflect difference in structuring of the bonded chains under dry and solvated conditions." @default.
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- W1991578049 date "1987-08-01" @default.
- W1991578049 modified "2023-09-27" @default.
- W1991578049 title "Effect of temperature on reversed-phase chromatographic surfaces studied by 13C NMR" @default.
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- W1991578049 doi "https://doi.org/10.1016/0022-2364(87)90086-2" @default.
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