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- W1991736469 abstract "Poly(N,N-dimethylacrylamide) (PDMA) with a low polydispersity was prepared via stable free radical polymerization (SFRP) using 2,2,6,6-tetramethyl-1-piperdinyloxy nitroxide (TEMPO). PDMA with a polydispersity of 1.55 (Mn = 10 600) was obtained for [TEMPO]/[AIBN] = 1.0 with quantitative monomer conversion; higher [TEMPO]/[AIBN] ratios decreased conversion. The polydispersity of PDMA was higher and polymerization times were shorter compared to SFRP of styrene or n-butyl acrylate. Attempts to prepare higher molecular weight PDMA with low polydispersity were unsuccessful. When polystyrene-TEMPO was used as a macroinitiator, N,N-dimethylacrylamide could be polymerized, but the conversion was low. Unlike styrene or acrylate polymerization, SFRP of N,N-dimethylacrylamide is not a living process, as evidenced by an unsuccessful incremental-monomer-addition experiment." @default.
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- W1991736469 date "1998-05-19" @default.
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- W1991736469 title "Synthesis of Poly(<i>N</i>,<i>N</i>-dimethylacrylamide) via Nitroxide-Mediated Radical Polymerization" @default.
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- W1991736469 doi "https://doi.org/10.1021/ma9716241" @default.
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