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• W1991994826 abstract "The reaction between (Me3Si)3CLi and BF3 in Et2O/THF gives the fluoride (Me3Si)3CB(F)[O(CH2)4C(SiMe3)3], which upon treatment with PhLi gives the corresponding phenyl compound (Me3Si)3CB(Ph)[O(CH2)4C(SiMe3)3]. A single crystal X-ray diffraction study has shown that in the latter the three bonds to boron lie in a plane, which is almost perpendicular to the plane of the Ph group. The CSiMe3 bonds (mean 1.900(12) Å) are probably longer than the SiMe bonds (mean 1.867(15) Å), and the CSiMe angles (mean 113.0(13)°) are larger than the MeSiMe angles (mean 105.6(12)°)." @default.
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• W1991994826 date "1982-09-01" @default.
• W1991994826 modified "2023-10-10" @default.
• W1991994826 title "The preparation and molecular structure of the highly sterically hindered tris(trimethylsilyl)methylboron compound (Me3Si)3CB(Ph)[O(CH2)4C(SiMe3)3]" @default.
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• W1991994826 doi "https://doi.org/10.1016/s0022-328x(00)96079-0" @default.
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