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• W1992008328 abstract "A 6Li NMR structural study of mixtures of labeled methyllithium, n-butyllithium, and 3-aminopyrrolidine lithium amide has been achieved in THF at −78 °C. In the first part, the study was focused on the mixed aggregates formed between methyllithium and n-butyllithium. The spectral data suggest that the two reactants form a series of tetramers (MeLi)4(n-BuLi)4−n, of which abundance depends on the proportion of the two alkyllithiums following a purely statistical distribution. The labeled chiral lithium amide was next introduced in the sample, and the competitive formation of the amide−methyllithium and amide−butyllithium mixed dimers was monitored in situ. The NMR spectra show a juxtaposition of signals typical of the entities characterized separately, suggesting that there is no preferential formation of one aggregate over the others." @default.
• W1992008328 created "2016-06-24" @default.
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• W1992008328 date "2008-06-25" @default.
• W1992008328 modified "2023-10-09" @default.
• W1992008328 title "⁶Li NMR Study of the Equilibrium between Methyllithium and <i>n</i>-Butyllithium in THF. Influence of a Third Partner, a Chiral Lithium Amide" @default.
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• W1992008328 doi "https://doi.org/10.1021/om800260c" @default.
• W1992008328 hasPublicationYear "2008" @default.
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