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- W1992077823 abstract "Several P-H-functionalised phosphinocyclopentadienes and lithium salts thereof were prepared: 1-SiMe2PHCy-2,3,4,5-Me4C5H (1) (Cy=C6H11), Li2[(C5Me4)SiMe2PCy] (1a), Li[(C5H4)CMe2PHPh] (2) and Li2[(C5H4)CH2CH2PPh] (3). 1 was obtained from 1-SiMe2Cl-2,3,4,5-Me4C5H and LiPHCy. Treatment of 1 with MeLi yields the corresponding dilithio salt 1a. 6,6-Dimethylfulvene reacts with LiPHPh to give 2. The three-membered ring of spiro[2,4]hepta-4,6-diene is cleaved by LiPHPh. Successive treatment of the intermediate monolithio salt with MeLi gives 3. Compounds 1–3 were characterised spectroscopically (1H, 31P, 13C, 7Li NMR; IR)." @default.
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- W1992077823 date "1999-06-01" @default.
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- W1992077823 title "P-H-functionalised phosphinocyclopentadienes: 1-SiMe2PHCy-2,3,4,5-Me4C5H, Li2[(C5Me4)SiMe2PCy], Li[(C5H4)CMe2PHPh] and Li2[(C5H4)CH2CH2PPh]" @default.
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- W1992077823 doi "https://doi.org/10.1016/s0277-5387(99)00098-4" @default.
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