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• W1992087127 abstract "A novel microporous titanosilicate JLU-1 (JiLin University number-1) has been successfully synthesized in a SiO2−TiO2−Na2O−H2O−(TMA)2O system. It is found that the JLU-1 sample requires a relatively low alkalinity and appropriate titanium content. The products are indexed as triclinic, a = 13.043(6) Å, b = 12.538(3) Å, c = 17.022(6) Å, α = 79.05°, β = 115.00°, γ = 84.81°. The samples have been characterized by powder X-ray diffraction (XRD), 29Si magic-angle spinning (MAS) NMR, scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HREM), infrared spectroscopy (IR), differential thermal−thermogravimetric analysis (DT-TGA), and adsorption measurements. Factors such as the initial TiO2/SiO2, Na2O/SiO2, and TMABr/SiO2 molar ratios, crystallization temperature, and cations which dominate the hydrothermal synthesis of the product are discussed." @default.
• W1992087127 created "2016-06-24" @default.
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• W1992087127 date "2000-03-01" @default.
• W1992087127 modified "2023-09-24" @default.
• W1992087127 title "Synthesis and Characterization of a Novel Microporous Titanosilicate JLU-1" @default.
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• W1992087127 doi "https://doi.org/10.1021/cm990384w" @default.
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