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• W1992197622 abstract "The kinetics of deuteration of resorcinol in pure D2O were studied for the first time using a flow-through capillary tubular reactor with on-line, proton, and deuterium NMR detection at high temperatures and high pressure. The global rate constants for hydrogen/deuterium (H/D) exchange were determined from temperatures of 200−450 °C (723 K) at a pressure of ∼400 bar (the critical temperature and pressure of water are 374.2 °C and 218.3 bar, respectively). The H/D exchange rate in resorcinol (1,3-dihydroxybenzene) under these extreme conditions was determined using proton NMR as a function of the resorcinol residence time in a capillary tubular reactor, which also served as a high-pressure NMR cell. The 1H and 2H NMR results indicate that H/D exchange in resorcinol for the ring protons was observed at temperatures as low as 200 °C. The kinetics of H/D exchange in resorcinol and the activation energy was extracted from the experimental 1H NMR data." @default.
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• W1992197622 date "1999-12-09" @default.
• W1992197622 modified "2023-10-17" @default.
• W1992197622 title "Kinetics of Deuterium Exchange on Resorcinol in D₂O at High Pressure and High Temperature" @default.
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• W1992197622 doi "https://doi.org/10.1021/jp991192r" @default.
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