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• W1992332012 abstract "A systematic study of RScSb (R = rare earth) ternary alloys has been carried out by X-ray diffraction, optical and electron microscopy and microprobe analysis. As a result, the new equiatomic RScSb (R = La–Nd, Sm, Gd–Tm, Lu, Y) compounds have been identified. No formation of equiatomic 1:1:1 phases has been observed for Eu and Yb. It has been found the RScSb compounds crystallize in two different crystal structures. The phases formed by the lighter R (La–Nd, Sm) adopt the CeScSi-type (tetragonal tI12, I4/mmm, an ordered variant of the La2Sb-type), while the ones containing the heavier R (R = Gd–Tm, Lu, Y) crystallize with the CeFeSi-type (tetragonal tP6, P4/nmm, an ordered derivative of the Cu2Sb-type). The latter phases were expected to be dimorphic, thus suggesting they might be polymorphic having the CeScSi-type as the low-temperature form; however, no proof of this was found in the course of the present study. Besides the equiatomic compounds, the R3Sc2Sb3 phases have also been identified. They form from Gd-Tm, Lu, included Y, and crystallize in the β-Yb5Sb3-type (orthorhombic oP32, Pnma). The observed lattice parameters, unit cell volume and volume contraction, for both the series of compounds, decrease on going from La to Lu following the lanthanide contraction trend. First principles calculations pinpoint that the differences in the electronic structure are directly related to the differences in the crystal structures of these compounds." @default.
• W1992332012 created "2016-06-24" @default.
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• W1992332012 date "2014-02-01" @default.
• W1992332012 modified "2023-09-25" @default.
• W1992332012 title "Systematics and anomalies in formation and crystal structures of RScSb and R3Sc2Sb3 rare earth compounds" @default.
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• W1992332012 doi "https://doi.org/10.1016/j.jallcom.2013.10.197" @default.
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