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• W1992463669 abstract "Organochlorine, organophosphate pesticides and fungicides in fruits and vegetables were analyzed using disposable pipette extraction (DPX) followed by gas chromatography–mass spectrometry-selective ion monitoring (GC/MS-SIM). The intrinsic rapid mixing capabilities of DPX result in fast and efficient extractions, and eluates are concentrated by using minimal elution solvent volumes rather than solvent evaporation methods. Matrix-matched calibrations were performed with reversed phase mechanisms (DPX-RP), and the limits of detection (LOD) were determined to be lower than 0.1 μg/mL for all targeted pesticides in carrot and orange sample matrices. Coefficients of determination (r2) were greater than 0.995 for most studied pesticides. DPX-RP exhibited recoveries between 72 and 116% for nonpolar and slightly polar pesticides (log P > 2) with most of the recoveries over 88%. Only very polar pesticides (e.g., acephate, mathamidophos) were not extracted well using DPX-RP." @default.
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• W1992463669 date "2010-03-01" @default.
• W1992463669 modified "2023-10-09" @default.
• W1992463669 title "Disposable pipette extraction for the analysis of pesticides in fruit and vegetables using gas chromatography/mass spectrometry" @default.
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• W1992463669 doi "https://doi.org/10.1016/j.chroma.2010.01.047" @default.
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