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- W1992578706 abstract "Mechanochemical and subsequent heating processes to produce SrVO3 are studied, starting from a mixture of Sr(OH)2 and VmOn (2/5≦m/n≦2/3) by milling and heating in an ambient or reducing atmosphere. Single phase perovskite SrVO3 was obtained by firing the milled mixtures at 1300°C under reducing atmosphere with four dehydration steps via two intermediates, Sr2V2O7 and Sr8V8O25. The fourth dehydration step, corresponding to transformation of Sr8V8O25 to SrVO3, appears at around 1100°C by heating mixtures containing trivalent vanadium and milled in a reducing atmosphere. Dehydration of the mixtures was promoted by milling under N2–4% H2, due to reduction of precursors by hydrogen. The precursor from the mixture with III–V mixed-valent vanadium milled under N2–4% H2 is closer to the final product SrVO3 than any other precursors." @default.
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- W1992578706 date "1999-08-01" @default.
- W1992578706 modified "2023-10-18" @default.
- W1992578706 title "Formation of SrVO3 precursors from Sr(OH)2 and VmOn (2/5≦m/n≦2/3) by mechanical stressing under ambient or reducing atmosphere" @default.
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- W1992578706 doi "https://doi.org/10.1016/s0167-2738(99)00090-9" @default.
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