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- W1992742459 abstract "Amines with chain lengths between one and fifteen carbon atoms were determined accurately at sub ppm levels by direct sample injection into a gas chromatograph. The amines were dissolved in different solvents including water. The prerequisite for success was a suitable column (28% Pennwalt 223 with 4% KOH on Gas-Chrom R, 60–230°C), the use of nitrogen-sensitive detector (Varian TSD) and the addition of ammonia to all solutions prior to analysis. The ability of ammonia to suppress adsorption of amines on glass surfaces and on the column packing was demonstrated. The influence of solvent, column temperature and sample size on the chromatograms was studied. The decomposition of the packing when aqueous samples were injected was shown to cause interference at some column temperatures." @default.
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- W1992742459 date "1981-03-01" @default.
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- W1992742459 title "Trace analysisi of free amines by gas-liquid chromatography" @default.
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- W1992742459 doi "https://doi.org/10.1016/s0021-9673(00)82690-4" @default.
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