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- W1992904098 abstract "Large single crystals (500 × 80 μm) of the structure type AFI have been obtained at 170°C using a synthesis medium containing F− anions. The new as-synthesized phase [AlPO4]12 Pr4NF crystallizes in space group P6cc with a = 13.740(5) Å and c = 8.474(4) Å (Z = 1). The crystal structure has been refined to Rw = 0.042. The Pr4N+ cations are in the large 12-ring channels of the framework, their fourfold inversion axis coinciding with the sixfold axis of the lattice. The F− anions are located in the “wall” of the framework between two (Al,P)O4 4-rings. This unusual position could be confirmed by 31P MAS n.m.r. spectroscopy." @default.
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- W1992904098 date "1989-09-01" @default.
- W1992904098 modified "2023-10-15" @default.
- W1992904098 title "Synthesis and structure of the [AlPO4]12 Pr4NF molecular sieve with AFI structure" @default.
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- W1992904098 doi "https://doi.org/10.1016/0144-2449(89)90101-2" @default.
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