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- W1992968609 abstract "Protonolysis of the zirconium borohydride [(C5H4R)2Zr(BH4)2] (R = H, Me, SiMe3) with NHMe2PhBPh4 in THF leads to the corresponding cationic zirconium complex [(C5H4R)2Zr(BH4)(THF)]BPh4, and the structure of [(C5H4Me)2Zr(BH4)(THF)]BPh4 was determined. In the presence of phosphine, PMe2Ph, the formation of the cationic hydride [(C5H4R)2ZrH(PMe2Ph)2]BPh4 is observed by 1H and 31P NMR followed by a disproportionation and a redox reaction with [BPh4]-, giving the neutral [(C5H4R)2ZrH(μ-H)]2 and the cationic ZrIII species [(C5H4R)2Zr(PMe2Ph)2]BPh4 characterized by EPR spectroscopy and suggesting a probable pathway in the deactivation of cationic catalyst systems." @default.
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- W1992968609 date "1997-12-01" @default.
- W1992968609 modified "2023-10-01" @default.
- W1992968609 title "Disproportionation of Cationic Zirconium Complexes: A Possible Pathway to the Deactivation of Catalytic Cationic Systems" @default.
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- W1992968609 doi "https://doi.org/10.1021/om9701736" @default.
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