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• W1993096620 abstract "In this paper, the conversion of azoxystrobin in a strongly fluorescent degradation product by UV irradiation with quantitative purposes and its fluorimetric determination are reported for the first time. A multicommuted flow injection-solid phase spectroscopy (FI-SPS) system combined with photochemically-induced fluorescence (PIF) is developed for the determination of azoxystrobin in grapes, must and wine. Grape samples were homogenized and extracted with methanol and further cleaned-up by solid-phase extraction on C(18) silica gel. Wine samples were solid-phase extracted on C(18) sorbent using dichloromethane as eluent. Recoveries of azoxystrobin from spiked grapes (0.5-2.0 mg Kg(-1)), must (0.5-2.0 microg mL(-1)) and wine (0.5-2.0 microg mL(-1)) were 84.0-87.6%, 95.5-105.9% and 88.5-111.2%, respectively. The quantification limit for grapes was 0.021 mg Kg(-1), being within European Union regulations, and 18 microg L(-1) and 8 microg L(-1) for must and wine, respectively." @default.
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• W1993096620 date "2007-02-01" @default.
• W1993096620 modified "2023-10-18" @default.
• W1993096620 title "Determination of azoxystrobin residues in grapes, musts and wines with a multicommuted flow-through optosensor implemented with photochemically induced fluorescence" @default.
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• W1993096620 doi "https://doi.org/10.1016/j.aca.2006.11.076" @default.
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