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- W1993113312 abstract "Pyruvic acid semicarbazonato manganese(II) hydrate, Mn(C4H6N3O3)2 . H2O, has been prepared and its IR spectra and thermal decomposition (TG) have been investigated. The crystal structure was determined by X-ray diffraction analysis. The crystal is triclinic, space group P1BAR with unit cell dimension a = 8.916(2), b = 9.362(2), c = 10.067(2) angstrom, alpha = 101.92(3), beta = 91.25(2), gamma = 117.08(3)degrees and V = 725.6(7) angstrom3, Z = 2, D(c) = 1.644 g cm-3. The structure was solved by the heavy-atom technique from 3586 observed, independent reflections recorded at 293 K and refined to a final R = 0.053. The manganese atom has a distorted octahedral coordination with ONO donor sets from hydrazone ligands. The crystal structure contains one water molecule of crystallization. The tight hydrogen-bonding network in the crystal packing gives rise to high thermal stability of the complex." @default.
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- W1993113312 date "1993-01-01" @default.
- W1993113312 modified "2023-09-27" @default.
- W1993113312 title "The manganese(II) complex of a hydrazone ligand derived from pyruvic acid and semicarbazide—synthesis, properties and crystal structure" @default.
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- W1993113312 doi "https://doi.org/10.1016/s0277-5387(00)84590-8" @default.
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